: An innovative and versatile set-up for in situ and real time measures in an electrochemical cell is described. An original coupling between micro-Raman spectroscopy and atomic force microscopy enables one to collect data on opaque electrodes. This system allows for the correlation of topographic images with chemical maps during the charge exchange occurring in oxidation/reduction processes. The proposed set-up plays a crucial role when reactions, both reversible and non-reversible, are studied step by step during electrochemical reactions and/or when local chemical analysis is required.

A Combined Raman Spectroscopy and Atomic Force Microscopy System for In Situ and Real-Time Measures in Electrochemical Cells

Bussetti, Gianlorenzo;Menegazzo, Marco;Castiglioni, Chiara;Tommasini, Matteo;Lucotti, Andrea;Magagnin, Luca;Russo, Valeria;Li Bassi, Andrea;Siena, Martina;Guadagnini, Alberto;Grillo, Samuele;Del Curto, Davide;Duo, Lamberto
2023-01-01

Abstract

: An innovative and versatile set-up for in situ and real time measures in an electrochemical cell is described. An original coupling between micro-Raman spectroscopy and atomic force microscopy enables one to collect data on opaque electrodes. This system allows for the correlation of topographic images with chemical maps during the charge exchange occurring in oxidation/reduction processes. The proposed set-up plays a crucial role when reactions, both reversible and non-reversible, are studied step by step during electrochemical reactions and/or when local chemical analysis is required.
2023
HOPG intercalation
Raman spectroscopy
in situ AFM
solid–liquid interface
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Utilizza questo identificativo per citare o creare un link a questo documento: https://hdl.handle.net/11311/1234603
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