The title acid was prepd. from cyclohexanone. Cyclohexanone was treated with H2O2 in HClO4, water was added, and the org. phase was sepd. and added to TiCl3, CH2:CHCOMe, and Me2CO at room temp. to give 9-oxodecanoic acid. Similarly, 10-oxoundecanoic acid was prepd. from cycloheptanone
One-step synthesis of 9-oxodecanoic acid and its methyl ester; a useful starting material for prostaglandin synthesis
CITTERIO, ATTILIO;VISMARA, ELENA
1980-01-01
Abstract
The title acid was prepd. from cyclohexanone. Cyclohexanone was treated with H2O2 in HClO4, water was added, and the org. phase was sepd. and added to TiCl3, CH2:CHCOMe, and Me2CO at room temp. to give 9-oxodecanoic acid. Similarly, 10-oxoundecanoic acid was prepd. from cycloheptanoneFile in questo prodotto:
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